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Beilstein J. Org. Chem. 2024, 20, 452–459, doi:10.3762/bjoc.20.40
Graphical Abstract
Scheme 1: Synthesis of 2,3-dibromo-1,1,1,4,4,4-hexafluorobutane (2).
Scheme 2: Synthesis of (E)-butene 3a.
Scheme 3: Isomerization reaction of (E)-butene 3a to (Z)-butene 3b.
Scheme 4: Synthesis of 2-chloro-3-iodo-1,1,1,4,4,4-hexafluorobutane (5).
Scheme 5: Dehydrohalogenation reaction of 2-chloro-3-iodo-1,1,1,4,4,4-hexafluorobutane (5).
Scheme 6: The reaction of silane 8 with I2/KF.
Scheme 7: The reaction of 3a with iPrMgCl and 4-fluorobenzaldehyde (9).
Scheme 8: The reaction of olefin 3a with iPrMgCl.
Scheme 9: The reaction of (E)-butene 3a with BuLi.
Scheme 10: The reaction of allene 11 with bromine.
Scheme 11: The reaction of allene 11 with ICl.
Scheme 12: Synthesis of 2,3-dibromo-2-chloro-1,1,1,4,4,4-hexafluorobutane (16).
Scheme 13: Synthesis of (Z, E)-2-bromo-3-chloro-1,1,1,4,4,4-hexafluorobut-2-enes (17a,b).
Scheme 14: The reaction of olefins 17a,b with BuLi.